Public Lab Wiki documentation



MiniVol TAS Particulate Matter Monitor



Table of Contents

What is the Minivol TAS?

What kinds of monitoring can the MiniVol do?

How is MiniVol used?

Lending

Get involved

FAQ

What is the MiniVol TAS?

The MiniVol Tactical Air Sampler is a low-volume, battery powered, filter-based Particulate Matter (PM) sampler developed by Airmetrics. In filter-based samplers, size-sorted particles are captured on a filter that is then weighed ('gravimetric analysis') to determine the concentration of particulate matter in the air pumped through the monitor (see more in the wiki). The MiniVol is designed for 24-hour samples that correspond with Federal Reference Method (FRM) monitors, but due to their lower air volume are not considered FRM-grade.

Public Lab has two MiniVols that can be loaned out for monitoring.

The MiniVol comes with chargers, outdoor mounts, and consumables neatly mounted inside its shipment-ready box:

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Outdoor mounts:

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Clockwise from top: Minivol, PM2.5 impactor, PM10 impactor, manual, battery pack.

How the MinVol works

The minivol has two different impactors, one for PM2.5, and one for PM10 (pictured up top, on the right). Impactors work to inertially sort particles:

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The MiniVol impactor:

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Because the MiniVol uses filters and an impactor, it must have the grease on its impactor plate replaced and cleaned every five sample periods, and it requires a new filter for every sample.

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What kinds of monitoring can the MiniVol do?

The MiniVol usually collects Particulate Matter (PM) on a filter for analysis. Tedlar bags can also be attached and used to collect gasses as well.

The MiniVol is designed for monitoring PM10 or PM2.5 over 24 hours. It cannot measure both PM10 and PM2.5 at the same time. Filters may be subjected to different types of analysis to speciate (identify) what the PM is made of.

The MiniVol samples a smaller volume of air than a Federal Reference Method monitor and has the best correspondence with FRMs at moderate-high PM concentrations.

Available types of analysis for MiniVol filters

Gravimetric -- Gravimetric analysis yields information about the total mass of particulates captured on the filter. Combined with the information about the volume of air that was sampled in order to collect those particles (which is determined using the pumping rate and the sampling time), gravimetric analyses provide information about the concentration of particulate matter in the air sampled. These results will be provided in mass per volume units-- usually micrograms per cubic meter of air-- and are comparable to national ambient air quality standards for particulate matter. Please note that the MiniVol can’t be used to conduct NAAQS enforceable monitoring, but the data types produced can be compared. Gravimetric analyses do not provide information about the composition of particles collected.

X-ray fluorescence -- X-ray fluorescence (XRF) analysis provides information about the elemental composition of the sample collected. This technique is useful if you want to know, for example, the total lead concentration but don’t need to know the speciation molecular form of it. For XRF, the sample is usually melted to create a homogeneous mixture. An x-ray beam is targeted at the melted sample, and its energy is absorbed by the sample, with various atoms becoming excited and kicking electrons to higher valence orbitals. Each atom has a characteristic energy associated with its excitation, and its relaxation. The energy of a sample’s relaxation is measured during XRF, and software is used to disambiguate the combination of elements that created that spectrum. XRF analysis can provide the concentration of various elements in a sample, though it cannot provide information about minerals. Labs can assess the silicon concentration alone, or provide information about a suite of metals. Note that silicon is the second most common element in Earth’s crust, so it is not likely to be a useful assessment if trying to determine a unique source contribution. Ratios of metals concentrations can often, though not always, yield information about particulate matter provenance. Metals concentrations may be more useful to provide a foundation for further risk assessment.

X-ray diffraction -- X-ray diffraction (XRD) analysis can provide information about the mineral structures in the sample collected. This technique is useful if you are interested in learning about the minerals and inorganic components of a sample, such as various types of crystalline silica. To conduct XRD analyses, a sample is ground into a fine powder, but not melted as it would be for XRF. In XRD, the sample powder is exposed to an incident x-ray beam, and resulting diffracted x-rays are their intensity is measured. Each crystalline lattice structure has characteristic molecular orbital spacing and orientation, which dictate the wavelength and directionality of resulting x-rays. Thus, minerals present in the sample can be uniquely identified by measuring the compilation of resulting x-rays. Labs commonly quantify the quartz present in a sample, as quartz is one of the most common minerals in Earth’s crust. Many labs can also quantify other forms of silica, including cristobalite and tridymite. Cristobalite and tridymite are both polymorphs of silica that form under high-temperature and are present in volcanic rocks. All three minerals (quartz, cristobalite, and tridymite) can be present in particles less than 4 micrometers in diameter and be considered respirable crystalline silica. Quartz is significantly more abundant than cristobalite or tridymite in most environments, and may comprise the majority of respirable crystalline silica in most samples.

Laboratory Services

Filters may be subject to several different types of analysis. Different analysis procedures require different types of filters, and the analysis procedure must be decided ahead of time.

Gravimetric analysis (weighing the filter) is the most basic analysis to which other procedures are added.

Analysis Filter Cost Lab(s)
Gravimetric Analysis (NIOSH 500) PTFE Filter, PVC Filter $20, $25 pre-loaded in cassettes ($30 fee for lost cassettes) Chester LabNET, Bureau Veritas
XRF for total Silicon PFTE Filter $30 +Gravimetric analysis Chester LabNET
XRF for metals (38 metals) PTFE Filter $70 +Gravimetric Analysis Chester LabNET
XRD for Quartz PVC filter (must be loaded into cassettes manually) $65 +Gravimetric Analysis Bureau Veritas
XRD for Quartz, Cristobalite PVC filter (must be loaded into cassettes manually) $75 +Gravimetric Analysis Bureau Veritas
XRD for Quartz, Cristobalite and Tridymite (NIOSH 7500) PVC filter (must be loaded into cassettes manually) $85 +Gravimetric Analysis Bureau Veritas

Prices quoted here are estimates and do not reflect actual lab prices.

Lab contact information:

  • Chester LabNET, 12242 SW Garden Place, Tigard OR 97223. Phone: 503.624.2183
  • Bureau Veritas, 22345 Roethel Drive, Novi MI 48375. Phone: 248.344.2671

Labs for organic/gas analysis:

how is the MiniVol used?

To deploy a MiniVol requires several steps outlined in the activities below.

  • The MiniVol requires maintenance: once-yearly calibration and a cleaning every five sampling periods.
  • To deploy the MiniVol in the field requires identifying a monitoring site and installation location, pre-deployment preparation, deployment, and analysis of laboratory results.
  • Many calculations in the activities require calculations. All equations in the MiniVol manual are implemented in the Open Document Format spreadsheet MiniVol Calibration.
  • Versions of this spreadsheet updated with the current calibration specific to each MiniVol are available on their equipment wiki pages (below in Lending).

__ MiniVol_calibration.ods

The spreadsheet was created with LibreOffice

The Field Data Sheet is used to record PM readings.

Lending

The Public Lab non-profit has two MiniVols available to loan:


The MiniVol TAS manual is available for download on the Airmetrics website

Get involved

Help out -- look at the activities below to learn how to try these techniques out, and the questions section for some of our as-yet unsolved challenges. Post your own questions to help flesh out this documentation.

Activities

Purpose Category Status Author Time Difficulty Replications
Routine maintenance and calibration of the MiniVol, with images - - @mathew - - 0 replications: Try it »
Identifying a PM monitoring site for deploying a MiniVol - - @mathew - - 1 replications: Try it »
MiniVol pre-deployment preparation, with images - - @mathew - - 1 replications: Try it »
MiniVol pre-deployment preparation, Updated - - @mathew - - 0 replications: Try it »
MiniVol pre-deployment preparation - - @mathew - - 1 replications: Try it »
Minivol PM monitoring deployment - - @mathew - - 0 replications: Try it »
Routine maintenance and calibration of the MiniVol - - @mathew - - 1 replications: Try it »
Troubleshooting leaks on the MiniVol - - @mathew - - 0 replications: Try it »

Add an activity  or request an activity

Activities should include a materials list, costs and a step-by-step guide to construction with photos. Learn what makes a good activity here.


Questions

Title Author Updated Likes
Can MiniVol (TAS Particulate Matter Monitor) measure Black Carbon or Elemental Carbon? @stevie about 1 month ago
Can PM4 be monitored with the MiniVol? @mathew over 1 year ago
What procedure is best to determine background airborne silica levels? @mathew over 1 year ago
calibration calculations don't match MiniVol manual @mathew over 1 year ago

Ask a question  or help answer future questions


methodologies dust silica pm particle-sensing pm-monitoring pm-sensing minivol method oil-and-gas airmetrics

method:oil-and-gas