Hey Guys, So I wanted to use the spectrometer to Characterize Carbon Nanotubes. I used a 50 W halogen lamp and follwed the procedure as given in the manual of the DIY spectrometer by Public Labs. However, I am not able to achieve a sharp spectrum. I have tried: 1) Changing the angle of inclination of the gumstick camera 2) changing the diffraction grating 3) changing the distance between the grating and the slit 4) changing the focus of the gumstick camera Despite changing the bove mentioned parameters, I havent achieved satisfactory results. I have attached a picture of the spectrum I've got so far. Would like to know where is the problem and how to rectify it.
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Hi, Ankur - nice spectrum. What would be an example of "ideal" results for you -- i just want to better understand exactly what you mean by sharp. Also, if you could link to your spectrum that would be helpful.
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Well There is a lot of blurring in the diffraction pattern that is formed.Also I have used the 0.12 mm collimated acetone slit. There is also a lot of overexposure of light and hence not giving an accurate spectrum. Since I am analysing Carbon Nanotubes, I need a well resloved spectrum inorder to find out absorbtion of specific wavelength. By Sharp I mean, that : A) Resolution of the pattern is better. B) No overexposure in certain regions of the spectrum C) No Blurring of the spectrum image I have attached a picture of absorbance graph of Carbon Nanotubes analysed by the Beckman Coulter DelsaMax PRO and one taken by Public lab spectrometer The picture shown below is by DelsaMax PRO
The picture shown below is by Public Lab spectrometer
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Hi, Ankur -
What is your hoped-for resolution? Can you link to your actual data on SpectralWorkbench.org so we can take a look? One way to determine what resolution you're getting is to look at a fluorescent (CFL) lightbulb spectrum. @cfastie has published a couple notes on very high resolution mods of the basic PL spectrometer design -- and his suggestions were used to dramatically improve the v3.0 spectrometer:
http://publiclab.org/notes/cfastie/1-21-2013/spectrometer-image-quality http://publiclab.org/notes/cfastie/2-19-2013/ebert
You can use an attenuator, as @stoft has described: http://publiclab.org/notes/stoft/05-14-2013/in-search-of-spectrometer-attenuators - and also see his other research for gain correction and a proposal for HDR exposure correction.
I think this is related to the first issue, but if there's a separate issue, can you elaborate?
Thanks for your input, Ankur! As with Chris Fastie's and Dave Stoft's suggestions, any improvements you can propose will be considered in upcoming revisions of the spectrometer kit design. We need all the input we can get -- that's how open source design works!
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